C₃₅H₆₄O₆

Base Information

Chemical Name:C₃₅H₆₄O₆
CAS No.:1449472-04-1
Molecular Formula:C₃₅H₆₄O₆
Molecular Weight:580.89
Hs Code.:

C<sub>35</sub>H<sub>64</sub>O<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₆₄O₆

Chemical Property:

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Technology Process of C₃₅H₆₄O₆

There total 17 articles about C₃₅H₆₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1449472-15-4
(S)-3-((2R,8S,Z)-2,8-bis((tert-butyldimethylsilyl)oxy)-14-((4R,5R)-2,2-dimethyl-5-tetradecyl-1,3-dioxolan-4-yl)tetradec-11-en-1-yl)-5-methylfuran-2(5H)-one

: 1449472-04-1
C₃₅H₆₄O₆

Guidance literature:: With acetyl chloride; In methanol; at 20 ℃; for 24h;
DOI:10.1002/anie.201208403

Reference yield:

: 112-71-0
1-Bromotetradecane

: 1449472-04-1
C₃₅H₆₄O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: magnesium; iodine / diethyl ether / 2 h / 20 °C

1.2: 2 h / 0 - 20 °C

2.1: propionic acid / benzene / 2 h / 150 °C

3.1: methanesulfonamide; AD-mix β / tert-butyl alcohol; water / 19 h / 0 °C

4.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 °C / Reflux

5.1: toluene-4-sulfonic acid / toluene / 60 °C

6.1: 1H-imidazole; iodine / dichloromethane / 2.5 h / 0 - 20 °C

7.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 - 20 °C

7.2: -78 - 20 °C

8.1: sec.-butyllithium; (-)-sparteine / tert-butyl methyl ether; cyclohexane / 5 h / -78 °C

8.2: 21 h / -78 °C / Reflux

9.1: 1H-imidazole / dichloromethane / 20 °C

10.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -78 - 0 °C

10.2: 3 h / 20 °C

11.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 h / 0 °C

12.1: acetyl chloride / methanol / 24 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; methanesulfonamide; AD-mix β; iodine; sec.-butyllithium; sodium hexamethyldisilazane; toluene-4-sulfonic acid; magnesium; propionic acid; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; (-)-sparteine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; tert-butyl methyl ether; cyclohexane; water; toluene; tert-butyl alcohol; benzene; 2.1: |Johnson-Claisen Rearrangement / 7.1: |Wittig Olefination / 7.2: |Wittig Olefination;
DOI:10.1002/anie.201208403

Reference yield:

: 909270-38-8
(E)-ethyl nonadec-4-enoate

: 1449472-04-1
C₃₅H₆₄O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: methanesulfonamide; AD-mix β / tert-butyl alcohol; water / 19 h / 0 °C

2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 °C / Reflux

3.1: toluene-4-sulfonic acid / toluene / 60 °C

4.1: 1H-imidazole; iodine / dichloromethane / 2.5 h / 0 - 20 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 - 20 °C

5.2: -78 - 20 °C

6.1: sec.-butyllithium; (-)-sparteine / tert-butyl methyl ether; cyclohexane / 5 h / -78 °C

6.2: 21 h / -78 °C / Reflux

7.1: 1H-imidazole / dichloromethane / 20 °C

8.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -78 - 0 °C

8.2: 3 h / 20 °C

9.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 h / 0 °C

10.1: acetyl chloride / methanol / 24 h / 20 °C

With 1H-imidazole; lithium aluminium tetrahydride; methanesulfonamide; AD-mix β; iodine; sec.-butyllithium; sodium hexamethyldisilazane; toluene-4-sulfonic acid; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; (-)-sparteine; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; tert-butyl methyl ether; cyclohexane; water; toluene; tert-butyl alcohol; 5.1: |Wittig Olefination / 5.2: |Wittig Olefination;
DOI:10.1002/anie.201208403