4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

Base Information

Chemical Name:4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid
CAS No.:75266-58-9
Molecular Formula:C₂₄H₃₆N₂O₆
Molecular Weight:448.56
Hs Code.:

4-Methyl-3-<4'β-<<<N'-<(tert-butyloxy)carbonyl>-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

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Technology Process of 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

There total 2 articles about 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 598-23-2
3-methyl-but-1-yne

: 75266-58-9,75266-59-0
4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-butyllithium

2: 1) KH, 2) H₂ / 2) 10percent Pd/C / 1) THF; 0 deg C to room temp., 1h, 2) THF, 37h, 20 psi

With n-butyllithium; hydrogen; potassium hydride; palladium on activated charcoal;
DOI:10.1021/jo01312a001

Reference yield:

: 68898-89-5
N,N'-tert-Butoxycarbonyl-L-prolyl-2-(4'-hydroxyphenyl)-ethylamin

: 75266-54-5
Benzyl 4-Methyl-2-pentynoate

: 75266-58-9,75266-59-0
4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

Guidance literature:: With hydrogen; potassium hydride; palladium on activated charcoal; Yield given. Multistep reaction; 1) THF; 0 deg C to room temp., 1h, 2) THF, 37h, 20 psi;
DOI:10.1021/jo01312a001