11-bromotricyclo<4.4.1.0^1,6>undeca-3,8-diene

Base Information

• Chemical Name: 11-bromotricyclo<4.4.1.0^1,6>undeca-3,8-diene
• CAS No.: 4622-37-1
• Molecular Formula: C₁₁H₁₃Br
• Molecular Weight: 225.128

Synonyms:

Chemical Property of 11-bromotricyclo<4.4.1.0^1,6>undeca-3,8-diene

Chemical Property:

Purity/Quality:

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Technology Process of 11-bromotricyclo<4.4.1.0^1,6>undeca-3,8-diene

There total 1 articles about 11-bromotricyclo<4.4.1.0^1,6>undeca-3,8-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

11,11-Dibromo-tricyclo<4.4.1.01,6>undeca-3,8-diene (4578-96-5) → 4-methylazulene (17647-77-7) + 11-bromotricyclo<4.4.1.01,6>undeca-3,8-diene (4622-37-1) + 1,6-methano[10]annulene (2443-46-1)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; Ambient temperature;

DOI:10.1039/c39810001182

Reference yield:

11-bromotricyclo<4.4.1.01,6>undeca-3,8-diene (4622-37-1) → 1,6-methano[10]annulene (2443-46-1)

Guidance literature:

With silver nitrate; In methanol; at 100 ℃;

DOI:10.1021/jo00865a002

Reference yield:

11-bromotricyclo<4.4.1.01,6>undeca-3,8-diene (4622-37-1) → Bicyclo<4.4.1>undeca-1,3,5,8-tetraen (6074-99-3)

Guidance literature:

With silver nitrate; In methanol; at 100 ℃;

DOI:10.1021/jo00865a002

upstream raw materials:

11,11-Dibromo-tricyclo<4.4.1.0^1,6>undeca-3,8-diene

Downstream raw materials:

Bicyclo<4.4.1>undeca-1,3,5,8-tetraen

1,6-methano[10]annulene

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