trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II)

Base Information

Chemical Name:trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II)
CAS No.:514848-10-3
Molecular Formula:C₁₁₄H₁₂₈Cl₂O₁₀P₄Pd
Molecular Weight:1959.49
Hs Code.:

trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II)

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Technology Process of trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II)

There total 1 articles about trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 12107-56-1
dichloro(1,5-cyclooctadiene)palladium(II)

: 514797-39-8
5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ₃-phosphorustrioxy)calix[4]arene

: 514848-10-3
trans-dichlorobis[5,11,17,23-tetra-tert-butyl-25-(diphenylphosphinoylmethoxy)-26,27,28-(μ3-phosphorustrioxy)calix[4]arene]-palladium(II)

Guidance literature:: In dichloromethane; N2; addn. of ligand to dichloromethane soln. of Pd complex, stirring for1 h; concn. under vac., pptn. by addn. of pentane and cooling to -20°C; elem. anal.;
DOI:10.1039/b204604k