O₂NC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄NO₂

Base Information

Chemical Name:O₂NC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄NO₂
CAS No.:860293-67-0
Molecular Formula:C₂₂H₄₄B₈N₆O₄
Molecular Weight:543.117
Hs Code.:

O<sub>2</sub>NC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>NH(CH<sub>2</sub>)4NH<sub>2</sub>(B<sub>8</sub>H<sub>11</sub>)NH(CH<sub>2</sub>)4NHCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>

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Chemical Property of O₂NC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄NO₂

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Technology Process of O₂NC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄NO₂

There total 1 articles about O₂NC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 860026-68-2
H₃BNH₂(CH₂)4NH₂

: 484050-03-5
(4-aminobutylamine)-(N-aminobutyl)azanonaborane⁽¹¹⁾

: 555-16-8
4-nitrobenzaldehdye

: 860293-67-0
O₂NC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄NO₂

Guidance literature:: In tetrahydrofuran; carbonyl compd. was added dropwise to soln. of azanonaborane and H3BNH2(CH2)4NH2 in THF at room temp.; mixt. was stirred for 2 d; filtered; volatiles removed (vac.); chromd. (silica gel, THF/CH2Cl2, 1/2); elem. anal.;
DOI:10.1039/b503445k