(E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate

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Chemical Name:(E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate
CAS No.:1420042-15-4
Molecular Formula:C₃₆H₂₈ClN₂O₂S₃*F₆P
Molecular Weight:797.246
Hs Code.:

(E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate

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Chemical Property of (E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate

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Technology Process of (E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate

There total 3 articles about (E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006-99-1
2-methyl-5-chloro-benzothiazole

: 1420042-15-4
(E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetonitrile / 5 h / Inert atmosphere; Microwave irradiation

2.1: N-ethyl-N,N-diisopropylamine / ethanol / 20 h / 20 °C

3.1: sodium hydroxide / ethanol; water / 0.08 h / Heating

3.2: 20 °C

4.1: butan-1-ol; toluene / 5 h / Reflux; Dean-Stark

With N-ethyl-N,N-diisopropylamine; sodium hydroxide; In ethanol; water; toluene; acetonitrile; butan-1-ol;
DOI:10.1021/ja3122312

Reference yield:

: 33599-35-8
5-chloro-3-ethyl-2-methylbenzothiazol-3-ium iodide

: 1420042-15-4
(E)-2-((E)-(5-chloro-3-ethylbenzothiazol-2(3H)-ylidene)methyl)-4-((5-(diphenylsulfonio)-3-ethylbenzothiazol-3-ium-2-yl)methylene)-3-oxocyclobut-1enolate hexafluorophosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / ethanol / 20 h / 20 °C

2.1: sodium hydroxide / ethanol; water / 0.08 h / Heating

2.2: 20 °C

3.1: butan-1-ol; toluene / 5 h / Reflux; Dean-Stark

With N-ethyl-N,N-diisopropylamine; sodium hydroxide; In ethanol; water; toluene; butan-1-ol;
DOI:10.1021/ja3122312