C₃₀H₄₂O₈S

Base Information

Chemical Name:C₃₀H₄₂O₈S
CAS No.:1373885-44-9
Molecular Formula:C₃₀H₄₂O₈S
Molecular Weight:562.725
Hs Code.:

C<sub>30</sub>H<sub>42</sub>O<sub>8</sub>S

Synonyms:

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Chemical Property of C₃₀H₄₂O₈S

Chemical Property:

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Technology Process of C₃₀H₄₂O₈S

There total 16 articles about C₃₀H₄₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₆O₆

: 98-59-9
p-toluenesulfonyl chloride

: 1373885-44-9
C₃₀H₄₂O₈S

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 120h;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: C₁₈H₂₈O₅

: 1373885-44-9
C₃₀H₄₂O₈S

Guidance literature:: Multi-step reaction with 11 steps

1: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

2: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

3: methanol; potassium carbonate / 15 h / 20 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

5: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

6: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 120 h / 20 °C

7: N-iodo-succinimide; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C

8: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 7 h / -40 - 20 °C

9: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

10: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

11: dmap; triethylamine / dichloromethane / 120 h / 0 - 20 °C

With 1H-imidazole; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; N-iodo-succinimide; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; water; zinc trifluoromethanesulfonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; 2: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: 81470-73-7
ethyl (4R,2E)-5-(benzyloxy)-4-methylpent-2-enoate

: 1373885-44-9
C₃₀H₄₂O₈S

Guidance literature:: Multi-step reaction with 17 steps

1: AD-mix-α; methanesulfonamide; water / tert-butyl alcohol / 72 h / 0 °C

2: pyridinium p-toluenesulfonate / dichloromethane; acetone / 10 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

4: 1H-imidazole; iodine; triphenylphosphine / toluene / 20 h / 20 °C

5: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 4 h / -40 - 20 °C

6: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 72 h / 20 °C

7: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

8: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

9: methanol; potassium carbonate / 15 h / 20 °C

10: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

11: 1H-imidazole / dichloromethane / 5 h / 0 - 20 °C

12: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 120 h / 20 °C

13: N-iodo-succinimide; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C

14: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 7 h / -40 - 20 °C

15: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

16: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

17: dmap; triethylamine / dichloromethane / 120 h / 0 - 20 °C

With 1H-imidazole; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; N-iodo-succinimide; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; methanesulfonamide; AD-mix-α; tetrabutyl ammonium fluoride; water; iodine; pyridinium p-toluenesulfonate; zinc trifluoromethanesulfonate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 1: Sharpless asymmetric dihydroxylation / 8: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090