Technology Process of C15H23NO4
There total 3 articles about C15H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: zinc dibromide / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
1.2: 1.5 h / 0 °C / Inert atmosphere
2.1: trifluoroacetic acid / tetrahydrofuran; water / 15 h / Inert atmosphere
3.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
4.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
dimethylsulfide borane complex; triethylamine; trifluoroacetic acid; zinc dibromide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c3ob27390c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / tetrahydrofuran; water / 15 h / Inert atmosphere
2: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
3: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
dimethylsulfide borane complex; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c3ob27390c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
2: dimethylsulfide borane complex / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere
With
dimethylsulfide borane complex; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob27390c