Technology Process of C23H29N3O5
There total 5 articles about C23H29N3O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
DOI:10.1002/cmdc.201200210
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 18-crown-6 ether; potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C
2.1: hydrazine hydrate / methanol; dichloromethane / 3 h / 20 °C
2.2: 1 h / 20 °C
3.1: pyridine / ethanol / 5 h / 60 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C
5.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 20 °C
With
pyridine; 18-crown-6 ether; tetrabutyl ammonium fluoride; potassium carbonate; hydrazine hydrate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
5.1: Mitsunobu reaction;
DOI:10.1002/cmdc.201200210
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C
2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 20 °C
With
tetrabutyl ammonium fluoride; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
2: Mitsunobu reaction;
DOI:10.1002/cmdc.201200210
