Technology Process of C22H24Br4N2O4*ClH
There total 6 articles about C22H24Br4N2O4*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
2: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C
With
hydrogenchloride; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridinium bromochromate / acetic acid / 2 h / 40 °C
2: potassium carbonate / N,N-dimethyl-formamide / 36 h / 20 °C
3: bromine / chloroform / 2 h / 20 °C
4: hydrogen bromide; water / methanol / 48 h
5: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 4 h
6: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C
With
hydrogenchloride; pyridinium bromochromate; water; hydrogen bromide; bromine; potassium carbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
1,4-dioxane; methanol; chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.07.017
