p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate

Base Information

Chemical Name:p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate
CAS No.:75266-60-3
Molecular Formula:C₃₀H₃₉N₃O₈
Molecular Weight:569.655
Hs Code.:

p-Nitrophenyl 4-Methyl-3-<4'β-<<<N'-<(tert-butyloxy)-carbonyl>-L-prolyl>amino>ethyl>phenoxy>pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate

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Technology Process of p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate

There total 4 articles about p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75266-58-9,75266-59-0
4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoic acid

: 658-78-6
1-nitro-4-trifluoroacetoxy-benzene

: 75266-60-3,75266-61-4
p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate

Guidance literature:: In pyridine; for 14h; Ambient temperature;
DOI:10.1021/jo01312a001

Reference yield:

: 598-23-2
3-methyl-but-1-yne

: 75266-60-3,75266-61-4
p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-butyllithium

2: 1) KH, 2) H₂ / 2) 10percent Pd/C / 1) THF; 0 deg C to room temp., 1h, 2) THF, 37h, 20 psi

3: 95 percent / pyridine / 14 h / Ambient temperature

With n-butyllithium; hydrogen; potassium hydride; palladium on activated charcoal; In pyridine;
DOI:10.1021/jo01312a001

Reference yield:

: 68898-89-5
N,N'-tert-Butoxycarbonyl-L-prolyl-2-(4'-hydroxyphenyl)-ethylamin

: 75266-60-3,75266-61-4
p-Nitrophenyl 4-Methyl-3-<4'β-<<-L-prolyl>amino>ethyl>phenoxy>pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KH, 2) H₂ / 2) 10percent Pd/C / 1) THF; 0 deg C to room temp., 1h, 2) THF, 37h, 20 psi

2: 95 percent / pyridine / 14 h / Ambient temperature

With hydrogen; potassium hydride; palladium on activated charcoal; In pyridine;
DOI:10.1021/jo01312a001