Technology Process of C34H45F3N2O8
There total 5 articles about C34H45F3N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / acetonitrile / 0.5 h / 20 °C
2: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 24 h / 0 °C
3: dmap; triethylamine / dichloromethane / 0 - 20 °C
With
dmap; potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; triethylamine; potassium hexacyanoferrate(III);
In
dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol300954s
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C
1.2: 1 h / 0 °C
2.1: dmap / acetonitrile / 0.5 h / 20 °C
3.1: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 24 h / 0 °C
4.1: dmap; triethylamine / dichloromethane / 0 - 20 °C
With
dmap; potassium osmate(VI) dihydrate; methanesulfonamide; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; potassium hexacyanoferrate(III);
In
tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol300954s
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -78 °C
1.2: 4.08 h / -78 - -50 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C
2.2: 1 h / 0 °C
3.1: dmap / acetonitrile / 0.5 h / 20 °C
4.1: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 24 h / 0 °C
5.1: dmap; triethylamine / dichloromethane / 0 - 20 °C
With
dmap; potassium osmate(VI) dihydrate; methanesulfonamide; tetrabutyl ammonium fluoride; tert.-butyl lithium; potassium carbonate; triethylamine; potassium hexacyanoferrate(III);
In
tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol; pentane;
DOI:10.1021/ol300954s