threo-5,6-dodecanediol

Base Information

Chemical Name:threo-5,6-dodecanediol
CAS No.:109786-53-0
Molecular Formula:C₁₂H₂₆O₂
Molecular Weight:202.337
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of threo-5,6-dodecanediol

Chemical Property:

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Technology Process of threo-5,6-dodecanediol

There total 4 articles about threo-5,6-dodecanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109786-64-3
(5R,6R)-5-(Isopropoxy-dimethyl-silanyl)-dodecan-6-ol

: 70859-32-4,70859-33-5,109786-53-0
threo-5,6-dodecanediol

Guidance literature:: With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; for 12h; Yield given; Ambient temperature;
DOI:10.1021/jo00228a056

Reference yield:

: 629-05-0
n-octyne

: 70859-32-4,70859-33-5,109786-53-0
threo-5,6-dodecanediol

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) Et₃N

2: m-chloroperbenzoic acid (MCPBA) / CH₂Cl₂ / 12 h / Ambient temperature

3: BF₃*OEt₂ / hexane; tetrahydrofuran / 2 h / -78 °C

4: 30percent H₂O₂, KF, KHCO₃ / methanol; tetrahydrofuran / 12 h / Ambient temperature

With potassium fluoride; boron trifluoride diethyl etherate; dihydrogen peroxide; potassium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/jo00228a056

Reference yield:

: 111581-59-0
(E)-1-(isopropoxydimethylsilyl)-1,2-epoxyoctane

: 70859-32-4,70859-33-5,109786-53-0
threo-5,6-dodecanediol

Guidance literature:: Multi-step reaction with 2 steps

1: BF₃*OEt₂ / hexane; tetrahydrofuran / 2 h / -78 °C

2: 30percent H₂O₂, KF, KHCO₃ / methanol; tetrahydrofuran / 12 h / Ambient temperature

With potassium fluoride; boron trifluoride diethyl etherate; dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/jo00228a056