Chrysophanol 8-O-beta-D-glucopyranoside

Base Information

• Chemical Name: Chrysophanol 8-O-beta-D-glucopyranoside
• CAS No.: 67492-66-4
• Molecular Formula: C₂₁H₂₀O₉
• Molecular Weight: 416.384
• Mol file: 67492-66-4.mol

Synonyms:

Chemical Property of Chrysophanol 8-O-beta-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Chrysophanol 8-O-beta-D-glucopyranoside

There total 4 articles about Chrysophanol 8-O-beta-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3,4,5-Trihydroxy-benzoic acid (2R,3S,4S,5R,6S)-3,4,5-trihydroxy-6-(8-hydroxy-6-methyl-9,10-dioxo-9,10-dihydro-anthracen-1-yloxy)-tetrahydro-pyran-2-ylmethyl ester → Chrysophanol 8-O-beta-D-glucopyranoside (13241-28-6,67492-66-4)

Guidance literature:

With sodium methylate; In methanol; at 20 ℃; for 1h;

DOI:10.1016/S0968-0896(00)00215-7

Reference yield:

1-hydroxy-3-methyl-8-(tetra-O-acetyl-β-D-glucopyranosyloxy)-anthraquinone → Chrysophanol 8-O-beta-D-glucopyranoside (13241-28-6,67492-66-4)

Guidance literature:

With potassium hydroxide;

Reference yield:

Chrysophanol (481-74-3) → Chrysophanol 8-O-beta-D-glucopyranoside (13241-28-6,67492-66-4)

Guidance literature:

Multi-step reaction with 2 steps

1: silver oxide; quinoline

2: aqueous KOH-solution

With quinoline; potassium hydroxide; silver(l) oxide;

upstream raw materials:

Chrysophanol

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

Downstream raw materials:

Chrysophanol