3-iodo-4-methylthiophene

Base Information

• Chemical Name: 3-iodo-4-methylthiophene
• CAS No.: 16494-41-0
• Molecular Formula: C₅H₅IS
• Molecular Weight: 224.065
• Mol file: 16494-41-0.mol

Synonyms:

Chemical Property of 3-iodo-4-methylthiophene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3-Iodo-4-methylthiophene 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-iodo-4-methylthiophene

There total 3 articles about 3-iodo-4-methylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-4-methylthiophene (30318-99-1) → 3-iodo-4-methylthiophene (16494-41-0)

Guidance literature:

With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine; In butan-1-ol; at 130 ℃; for 40h;

Reference yield:

3-Methyl-2,4,5-triiodthiophen (16488-62-3) → 3-iodo-4-methylthiophene (16494-41-0)

Guidance literature:

With diethyl ether; magnesium; methyl iodide;

Reference yield:

3-Methylthiophene (616-44-4,84928-92-7) → 3-iodo-4-methylthiophene (16494-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: mercury (II)-acetate; acetic acid; iodine

2: magnesium; diethyl ether; methyl iodide

With diethyl ether; mercury(II) diacetate; iodine; magnesium; acetic acid; methyl iodide;

upstream raw materials:

3-Methyl-2,4,5-triiodthiophen

3-Methylthiophene

3-bromo-4-methylthiophene

Downstream raw materials:

4-methylthiophene-3-carboxylic acid