10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate

Base Information

Chemical Name:10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate
CAS No.:1430745-11-1
Molecular Formula:C₄H₄O₄*C₂₂H₂₃N₅O
Molecular Weight:489.531
Hs Code.:

Synonyms:

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Chemical Property of 10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate

Chemical Property:

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Technology Process of 10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate

There total 6 articles about 10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 934-32-7
1H-benzimidazol-2-amine

: 1430745-11-1
10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydroxide; potassium carbonate / acetone / 3 h / Reflux

2: sodium; ethanol / 3 h / 150 °C

3: hydrogenchloride; water

4: trichlorophosphate / 2 h / 130 °C

5: ethanol / 3 h / Reflux

6: ethanol

With hydrogenchloride; ethanol; water; sodium; potassium carbonate; potassium hydroxide; trichlorophosphate; In ethanol; acetone;
DOI:10.1016/j.ejmech.2013.01.026

Reference yield:

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 1430745-11-1
10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydroxide; potassium carbonate / acetone / 3 h / Reflux

2: sodium; ethanol / 3 h / 150 °C

3: hydrogenchloride; water

4: trichlorophosphate / 2 h / 130 °C

5: ethanol / 3 h / Reflux

6: ethanol

With hydrogenchloride; ethanol; water; sodium; potassium carbonate; potassium hydroxide; trichlorophosphate; In ethanol; acetone;
DOI:10.1016/j.ejmech.2013.01.026

Reference yield:

: 1430744-75-4
2-hydroxy-10-(1-phenylethyl)pyrimido[1,2-a]benzimidazol-4(10H)-one

: 1430745-11-1
10-(1-phenylethyl)-2-(1-piperazinyl)pyrimido[1,2-a]benzimidazol-4(10H)-one maleate

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 2 h / 130 °C

2: ethanol / 3 h / Reflux

3: ethanol

With trichlorophosphate; In ethanol;
DOI:10.1016/j.ejmech.2013.01.026