Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate

Base Information

Chemical Name:Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate
CAS No.:106696-09-7
Molecular Formula:C₂₃H₁₉NO₄
Molecular Weight:373.408
Hs Code.:

Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzo<f>quinolino-2-glyoxalate

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Chemical Property of Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate

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Technology Process of Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate

There total 4 articles about Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 106696-07-5
1-Oxo-4-phenyl-1,2,3,4-tetrahydrobenzo[f]quinoline

: 95-92-1
oxalic acid diethyl ester

: 106696-09-7
Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate

Guidance literature:: With sodium ethanolate; In benzene; for 7h; Ambient temperature;

Reference yield:

: 135-88-6,84420-28-0
N-Phenyl-2-naphthylamine

: 106696-09-7
Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / gl. acetic acid

2: 74 percent / alkaline hydrolysis

3: 60 percent / P₂O₅, phosphoric acid / 2 h / 100 °C

4: 65 percent / NaOC₂H₅ / benzene / 7 h / Ambient temperature

With phosphoric acid; sodium ethanolate; phosphorus pentoxide; acetic acid; In benzene;

Reference yield:

: N-(β-naphthyl)-N-(phenyl)-β-aminopropionitrile

: 106696-09-7
Ethyl 1-oxo-4-phenyl-1,2,3,4-tetrahydrobenzoquinolino-2-glyoxalate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / alkaline hydrolysis

2: 60 percent / P₂O₅, phosphoric acid / 2 h / 100 °C

3: 65 percent / NaOC₂H₅ / benzene / 7 h / Ambient temperature

With phosphoric acid; sodium ethanolate; phosphorus pentoxide; In benzene;