(2,2':6',2''-terpyridine-κ3N,N',N'')bis(triphenylphosphine-κP)copper(I) perchlorate

Base Information

Chemical Name:(2,2':6',2''-terpyridine-κ3N,N',N'')bis(triphenylphosphine-κP)copper(I) perchlorate
CAS No.:154294-07-2
Molecular Formula:C₅₁H₄₁CuN₃P₂*ClO₄
Molecular Weight:920.851
Hs Code.:

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Chemical Property of (2,2':6',2''-terpyridine-κ3N,N',N'')bis(triphenylphosphine-κP)copper(I) perchlorate

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Technology Process of (2,2':6',2''-terpyridine-κ3N,N',N'')bis(triphenylphosphine-κP)copper(I) perchlorate

There total 1 articles about (2,2':6',2''-terpyridine-κ3N,N',N'')bis(triphenylphosphine-κP)copper(I) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1148-79-4
2,2':6,2''-terpyridine

: 95401-72-2
[Cu(CH₃CN)₂(triphenylphosphine)₂]ClO₄

: 154294-07-2
(2,2':6',2''-terpyridine-κ3N,N',N'')bis(triphenylphosphine-κP)copper(I) perchlorate

Guidance literature:: In dichloromethane; under N2, addn. of terpy in CH2Cl2 to a CH2Cl2 soln. of the Cu complex, immediately turning yellow, addn. of ethanol, heating under N2 flow until crystn.; cooling to room temp., vac. filtration, washing (cold ethanol), drying in vac., elem. anal.;
DOI:10.1039/DT9940000215