1-boraadamantane o-tolunitrile complex

Base Information

• Chemical Name: 1-boraadamantane o-tolunitrile complex
• CAS No.: 90789-71-2
• Molecular Formula: C₁₇H₂₂BN
• Molecular Weight: 251.179
• Mol file: 90789-71-2.mol

Synonyms:

Chemical Property of 1-boraadamantane o-tolunitrile complex

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1-boraadamantane o-tolunitrile complex

There total 1 articles about 1-boraadamantane o-tolunitrile complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Methylbenzonitrile (529-19-1) + 1-boraadamantane (38673-97-1) → 1-boraadamantane o-tolunitrile complex (90789-71-2)

Guidance literature:

In hexane; soln. of o-tolunitrile in hexane added dropwise under Ar at 20 °Cto soln. of 1-boraadamantane in hexane; ppt. washed with hexane;

DOI:10.1016/S0022-328X(00)98669-8

Reference yield:

1-boraadamantane o-tolunitrile complex (90789-71-2) → (CH3C6H4C(C9H15B)N)2

Guidance literature:

In not given; heated under Ar;

DOI:10.1016/S0022-328X(00)98669-8

upstream raw materials:

2-Methylbenzonitrile

1-boraadamantane