Technology Process of C22H21Br3ClN3O2
There total 8 articles about C22H21Br3ClN3O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trichlorophosphate / N,N-dimethyl-formamide
2: caesium carbonate; sodium iodide / butanone
With
caesium carbonate; sodium iodide; trichlorophosphate;
In
N,N-dimethyl-formamide; butanone;
DOI:10.1016/j.bmcl.2012.12.033
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium acetate / ethanol
2: trichlorophosphate / N,N-dimethyl-formamide
3: caesium carbonate; sodium iodide / butanone
With
ammonium acetate; caesium carbonate; sodium iodide; trichlorophosphate;
In
ethanol; N,N-dimethyl-formamide; butanone;
DOI:10.1016/j.bmcl.2012.12.033
- Guidance literature:
-
Multi-step reaction with 8 steps
1: bromine / acetic acid / 2 h / 20 °C
2: bromine / chloroform / 2 h / 20 °C
3: chloroform / 18 h / 20 °C
4: hydrogen bromide / methanol / 48 h
5: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 4-methyl-morpholine / N,N-dimethyl-formamide / 2 h / 20 °C
6: ammonium acetate / ethanol
7: trichlorophosphate / N,N-dimethyl-formamide
8: caesium carbonate; sodium iodide / butanone
With
4-methyl-morpholine; ammonium acetate; hydrogen bromide; bromine; caesium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; sodium iodide; trichlorophosphate;
In
methanol; ethanol; chloroform; acetic acid; N,N-dimethyl-formamide; butanone;
2: |Delepine Amine Synthesis;
DOI:10.1016/j.bmcl.2012.12.033
