C₂₃H₂₉N₃O₈S

Base Information

Chemical Name:C₂₃H₂₉N₃O₈S
CAS No.:1449016-70-9
Molecular Formula:C₂₃H₂₉N₃O₈S
Molecular Weight:507.565
Hs Code.:

C<sub>23</sub>H<sub>29</sub>N<sub>3</sub>O<sub>8</sub>S

Synonyms:

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Chemical Property of C₂₃H₂₉N₃O₈S

Chemical Property:

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Technology Process of C₂₃H₂₉N₃O₈S

There total 8 articles about C₂₃H₂₉N₃O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449016-67-4
C₂₃H₂₉N₃O₆S

: 1449016-70-9
C₂₃H₂₉N₃O₈S

Guidance literature:: Multi-step reaction with 3 steps

1: sodium periodate; silica gel / acetonitrile; ethyl acetate / 24 h / 20 °C

2: dihydrogen peroxide; sodium chlorite / water; acetonitrile; aq. phosphate buffer / 0.75 h / 0 °C

3: dichloromethane; diethyl ether / 20 °C

With sodium chlorite; sodium periodate; dihydrogen peroxide; silica gel; In aq. phosphate buffer; diethyl ether; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1002/ejoc.201201516

Reference yield:

: 60410-16-4
(1R,4S)-4-hydroxy-2-cyclopentene-1-yl acetate

: 1449016-70-9
C₂₃H₂₉N₃O₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 0 - 20 °C

2.1: potassium carbonate; thiophenol / tetrahydrofuran; N,N-dimethyl-formamide / 3.5 h / 20 - 70 °C

2.2: 12 h / 60 °C

2.3: 12 h / 20 °C

3.1: potassium hydride; dibenzo-18-crown-6 / tetrahydrofuran / 20 °C

4.1: n-butyllithium / tetrahydrofuran / 17.5 h / -100 - -60 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 0 °C

6.1: Hoveyda-Grubbs catalyst second generation; ethene / dichloromethane / 24 h / -10 - 45 °C / 760.05 Torr / Inert atmosphere

7.1: AD-mix β; tert-butyl alcohol / water / 24 h / 0 °C

8.1: sodium periodate; silica gel / acetonitrile; ethyl acetate

9.1: dihydrogen peroxide; sodium chlorite / water; acetonitrile; aq. phosphate buffer / 0.75 h / 0 °C

10.1: dichloromethane; diethyl ether / 20 °C

With sodium chlorite; sodium periodate; dibenzo-18-crown-6; n-butyllithium; Hoveyda-Grubbs catalyst second generation; ethene; di-isopropyl azodicarboxylate; AD-mix β; dihydrogen peroxide; silica gel; potassium hydride; potassium carbonate; thiophenol; triphenylphosphine; tert-butyl alcohol; In tetrahydrofuran; aq. phosphate buffer; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: |Fukuyama Coupling / 3.1: |Williamson Ether Synthesis / 4.1: |Wittig Rearrangement / 5.1: |Fukuyama Coupling;
DOI:10.1002/ejoc.201201516

Reference yield:

: allyl-((1R,4R)-4-tributylstannanylmethoxy-cyclopent-2-enyl)-carbamic acid tert-butyl ester

: 1449016-70-9
C₂₃H₂₉N₃O₈S

Guidance literature:: Multi-step reaction with 6 steps

1: n-butyllithium / tetrahydrofuran / 17.5 h / -100 - -60 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 0 °C

3: Hoveyda-Grubbs catalyst second generation; ethene / dichloromethane / 24 h / -10 - 45 °C / 760.05 Torr / Inert atmosphere

4: sodium periodate; silica gel / acetonitrile; ethyl acetate / 24 h / 20 °C

5: dihydrogen peroxide; sodium chlorite / water; acetonitrile; aq. phosphate buffer / 0.75 h / 0 °C

6: dichloromethane; diethyl ether / 20 °C

With sodium chlorite; sodium periodate; n-butyllithium; Hoveyda-Grubbs catalyst second generation; ethene; di-isopropyl azodicarboxylate; dihydrogen peroxide; silica gel; triphenylphosphine; In tetrahydrofuran; aq. phosphate buffer; diethyl ether; dichloromethane; water; ethyl acetate; acetonitrile; 1: |Wittig Rearrangement / 2: |Fukuyama Coupling;
DOI:10.1002/ejoc.201201516