Technology Process of C25H27N3O3S
There total 6 articles about C25H27N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / ethanol; water / 3 h / Reflux
1.2: 0.5 h / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 20 °C
3.1: chlorosulfonic acid / chloroform / 6 h / 0 - 50 °C
4.1: base / 20 °C
With
chlorosulfonic acid; sodium hydride; sodium hydroxide;
In
ethanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.065
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydroxylamine hydrochloride; pyridine / 1 h / 95 °C
2.1: 1 h / 95 °C
3.1: sodium hydroxide / ethanol; water / 3 h / Reflux
3.2: 0.5 h / 20 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 20 °C
5.1: chlorosulfonic acid / chloroform / 6 h / 0 - 50 °C
6.1: base / 20 °C
With
pyridine; chlorosulfonic acid; hydroxylamine hydrochloride; sodium hydride; sodium hydroxide;
In
ethanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.065
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / N,N-dimethyl-formamide / 3 h / 0 - 20 °C
2: chlorosulfonic acid / chloroform / 6 h / 0 - 50 °C
3: base / 20 °C
With
chlorosulfonic acid; sodium hydride;
In
chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.03.065