Technology Process of C19H27NO3
There total 3 articles about C19H27NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere
2: hydroxylamine hydrochloride; pyridine / Inert atmosphere
With
pyridine; hydroxylamine hydrochloride; Dess-Martin periodane;
In
dichloromethane;
1: |Dess-Martin Oxidation;
DOI:10.1021/ol501010k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere
3.1: hydroxylamine hydrochloride; pyridine / Inert atmosphere
With
pyridine; hydroxylamine hydrochloride; Dess-Martin periodane; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
2.1: |Dess-Martin Oxidation;
DOI:10.1021/ol501010k
- Guidance literature:
-
With
pyridine; hydroxylamine hydrochloride;
Inert atmosphere;
DOI:10.1021/ol501010k