Technology Process of Propanedinitrile,
2,2'-(2-hexadecyl-2,5-cyclohexadiene-1,4-diylidene)bis-
There total 3 articles about Propanedinitrile,
2,2'-(2-hexadecyl-2,5-cyclohexadiene-1,4-diylidene)bis- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
hexadecyl-1,4-cyclohexanedione; malononitrile;
With
3-amino propanoic acid;
In
tetrahydrofuran; water;
for 7h;
Heating;
With
N-Bromosuccinimide;
In
acetonitrile;
for 0.5h;
With
pyridine;
In
water; acetonitrile;
for 0.166667h;
DOI:10.1081/SCC-100103524
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diethylamine; lithium / tetrahydrofuran; hexamethylphosphoric acid triamide / 10 - 15 °C / ultrasonic irradiation
1.2: tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h
1.3: 41 percent / HCl / H2O; hexamethylphosphoric acid triamide / 2.5 h / Heating
2.1: β-alanine / tetrahydrofuran; H2O / 7 h / Heating
2.2: bromosuccinimide / acetonitrile / 0.5 h
2.3: 38 percent / pyridine / H2O; acetonitrile / 0.17 h
With
lithium; diethylamine; 3-amino propanoic acid;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; water;
DOI:10.1081/SCC-100103524
- Guidance literature:
-
With
N-Bromosuccinimide;
In
acetonitrile;
for 0.5h;
Yield given;
