Technology Process of N-(3-chlorophenyl)-4-phenoxybenzamide
There total 3 articles about N-(3-chlorophenyl)-4-phenoxybenzamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / 90 °C / Inert atmosphere
2: water; sodium hydroxide / ethanol / 3 h / Reflux
3: thionyl chloride / chloroform / 0.5 h / Reflux
4: triethylamine / dichloromethane / 0 - 20 °C
With
copper(l) iodide; thionyl chloride; dimethylaminoacetic acid; water; caesium carbonate; triethylamine; sodium hydroxide;
In
1,4-dioxane; ethanol; dichloromethane; chloroform;
1: Ullmann reaction;
DOI:10.1016/j.bmcl.2011.12.022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / 90 °C / Inert atmosphere
2: water; sodium hydroxide / ethanol / 3 h / Reflux
3: thionyl chloride / chloroform / 0.5 h / Reflux
4: triethylamine / dichloromethane / 0 - 20 °C
With
copper(l) iodide; thionyl chloride; dimethylaminoacetic acid; water; caesium carbonate; triethylamine; sodium hydroxide;
In
1,4-dioxane; ethanol; dichloromethane; chloroform;
1: Ullmann reaction;
DOI:10.1016/j.bmcl.2011.12.022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; sodium hydroxide / ethanol / 3 h / Reflux
2: thionyl chloride / chloroform / 0.5 h / Reflux
3: triethylamine / dichloromethane / 0 - 20 °C
With
thionyl chloride; water; triethylamine; sodium hydroxide;
In
ethanol; dichloromethane; chloroform;
DOI:10.1016/j.bmcl.2011.12.022
