Zr[tBu-ONPyrO]Bn₂

Base Information

Chemical Name:Zr[tBu-ONPyrO]Bn₂
CAS No.:329009-67-8
Molecular Formula:C₅₀H₆₄N₂O₂Zr
Molecular Weight:816.294
Hs Code.:

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Chemical Property of Zr[tBu-ONPyrO]Bn₂

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Technology Process of Zr[tBu-ONPyrO]Bn₂

There total 7 articles about Zr[tBu-ONPyrO]Bn₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24356-01-2
tetrabenzylzirconium(IV)

: 276866-85-4
N-(2-pyridylmethyl)-N,N-bis(2-hydroxy-3,5-di-tert-butylbenzyl)amine

: 329009-67-8,418758-42-6
(C₆H₅CH₂)2Zr(C₅H₄NCH₂N(CH₂C₆H₂(C(CH₃)3)2O)2)

Guidance literature:: In toluene; (N2); addn. of a soln. of ligand in toluene to a soln. of zirconium compd. in toluene at room temp., heating to 65°C, stirring for 2 h; evapn.;
DOI:10.1021/om0101285

Reference yield: 84.0%

: 24356-01-2
tetrabenzylzirconium(IV)

: 276866-85-4
N-(2-pyridylmethyl)-N,N-bis(2-hydroxy-3,5-di-tert-butylbenzyl)amine

: 329009-67-8,418758-42-6
Zr[tBu-ONPyrO]Bn₂

Guidance literature:: In toluene; at 60 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja401474v

Reference yield: 54.0%

: N-(2-pyridylmethyl)-N,N-bis(2'-hydroxy-3',5'-di(tert-butyl)benzyl)amine

: 24356-01-2
tetrabenzylzirconium(IV)

: 329009-67-8,418758-42-6
(C₆H₅CH₂)2Zr(C₅H₄NCH₂N(CH₂C₆H₂(C(CH₃)3)2O)2)

Guidance literature:: In benzene; a soln. of amine in benzene was added dropwise to a soln. of complex in benzene with cooling on ice/water bath, the mixt. was allowed to warm toroom temp. and stirred for 2 h with exclusion of light (inert atm.); extd. into ether, filtered, concd., cooled to -30°C; elem. anal.;
DOI:10.1021/om010982w