Technology Process of C13H19N3*ClH
There total 9 articles about C13H19N3*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / 14 h / 0 - 20 °C
2: dichloromethane / 20 °C
3: hydrogenchloride; sodium chloride / water
4: ammonia / methanol / 20 °C
5: hydrogen / ethanol / 20 °C
6: Raney Ni / butan-1-ol / 120 °C
7: hydrogenchloride / water
With
hydrogenchloride; di-isopropyl azodicarboxylate; ammonia; hydrogen; triphenylphosphine; sodium chloride;
In
methanol; ethanol; dichloromethane; water; toluene; butan-1-ol;
1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2014.01.021
- Guidance literature:
-
Multi-step reaction with 7 steps
1: triethylamine
2: dichloromethane / 20 °C
3: hydrogenchloride; sodium chloride / water
4: ammonia / methanol / 20 °C
5: hydrogen / ethanol / 20 °C
6: Raney Ni / butan-1-ol / 120 °C
7: hydrogenchloride / water
With
hydrogenchloride; ammonia; hydrogen; triethylamine; sodium chloride;
In
methanol; ethanol; dichloromethane; water; butan-1-ol;
DOI:10.1016/j.bmcl.2014.01.021
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dichloromethane / 20 °C
2: hydrogenchloride; sodium chloride / water
3: ammonia / methanol / 20 °C
4: hydrogen / ethanol / 20 °C
5: Raney Ni / butan-1-ol / 120 °C
6: hydrogenchloride / water
With
hydrogenchloride; ammonia; hydrogen; sodium chloride;
In
methanol; ethanol; dichloromethane; water; butan-1-ol;
DOI:10.1016/j.bmcl.2014.01.021
