(E)-diethyl 2-(2-formylphenyl)fumarate

Base Information

• Chemical Name: (E)-diethyl 2-(2-formylphenyl)fumarate
• CAS No.: 1586768-51-5
• Molecular Formula: C₁₅H₁₆O₅
• Molecular Weight: 276.289
• Mol file: 1586768-51-5.mol

Synonyms:

Chemical Property of (E)-diethyl 2-(2-formylphenyl)fumarate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-diethyl 2-(2-formylphenyl)fumarate

There total 1 articles about (E)-diethyl 2-(2-formylphenyl)fumarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-bromobenzaldehyde (6630-33-7) + 1,4-dimethyl but-2-enedioate (23055-10-9) → (E)-diethyl 2-(2-formylphenyl)fumarate (1586768-51-5) + diethyl 2-(2-formylphenyl)maleate (1586768-70-8)

Guidance literature:

With palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 110 ℃; for 12.5h; Overall yield = 39 %; Overall yield = 233.3 mg; Inert atmosphere;

DOI:10.1039/c3ob42546k

upstream raw materials:

ortho-bromobenzaldehyde

1,4-dimethyl but-2-enedioate

Refernces