dihydrido(η-mesitylene)(triisopropylphosphine)osmium(II)

Base Information

Chemical Name:dihydrido(η-mesitylene)(triisopropylphosphine)osmium(II)
CAS No.:131220-60-5
Molecular Formula:C₁₈H₃₅OsP
Molecular Weight:472.65
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dihydrido(η-mesitylene)(triisopropylphosphine)osmium(II)

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Technology Process of dihydrido(η-mesitylene)(triisopropylphosphine)osmium(II)

There total 1 articles about dihydrido(η-mesitylene)(triisopropylphosphine)osmium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 131220-50-3
chloro(hydrido)(η-mesitylene)(triphenylphosphine)osmium(II)

: 917-54-4
methyllithium

: 131220-45-6
dichloro(η-mesitylene)(triphenylphosphine)osmium(II)

: 131220-60-5
dihydrido(η-mesitylene)(triisopropylphosphine)osmium(II)

: OsCl(C₆H₄P(C₆H₅)2)(C₆H₃(CH₃)3)

Guidance literature:: With methanol; chloroform; In diethyl ether; chloroform; treatment with LiMe at -78°C, warming to room temperature with stirring, after 4h cooling to -78°C, treatment of the solid with CHCl3, refluxed for 1h; removal of solvent, chromatographed on alumina, evapn. to dryness, recrystn. from ether, NMR, IR, MS, elem. anal.;