bis(2,4,6-tri-tert-butylphenyl)phosphinimine

Base Information

• Chemical Name: bis(2,4,6-tri-tert-butylphenyl)phosphinimine
• CAS No.: 122691-32-1
• Molecular Formula: C₃₆H₅₈NP
• Molecular Weight: 535.837
• Mol file: 122691-32-1.mol

Synonyms:

Chemical Property of bis(2,4,6-tri-tert-butylphenyl)phosphinimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(2,4,6-tri-tert-butylphenyl)phosphinimine

There total 1 articles about bis(2,4,6-tri-tert-butylphenyl)phosphinimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-methylphenyl ester of N-<2,4,6-tri(tert-butyl)phenyl>imidophosphenous acid (122691-31-0) + 2,4,6-tri-tert-butylphenyllithium (35383-91-6) → bis(2,4,6-tri-tert-butylphenyl)phosphinimine (122691-32-1,160716-61-0)

Guidance literature:

In tetrahydrofuran; 1.) -78 deg C, 1 h, 2.) 25 deg C, 3 h;

Reference yield: 87.0%

bis(2,4,6-tri-tert-butylphenyl)phosphinimine (122691-32-1,160716-61-0) → C36H58NOP

Guidance literature:

With oxygen; ozone; In dichloromethane; at -78 ℃;

Reference yield: 72.0%

bis(2,4,6-tri-tert-butylphenyl)phosphinimine (122691-32-1,160716-61-0) → C36H59N4P (164358-67-2)

Guidance literature:

With methanol; trimethylsilylazide; for 12h; Ambient temperature;

upstream raw materials:

2-methylphenyl ester of N-<2,4,6-tri(tert-butyl)phenyl>imidophosphenous acid

2,4,6-tri-tert-butylphenyllithium

Downstream raw materials:

C₃₇H₅₈Cl₂NP

C₃₆H₅₉N₄P

C₃₇H₅₈ClLiNP

C₄₀H₆₇NP₂