Technology Process of C28H26O6
There total 11 articles about C28H26O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / methanol / 20 °C
2: N-Bromosuccinimide; silver nitrate / acetone / 1.5 h / 20 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
4: N-Bromosuccinimide; silver fluoride / acetonitrile / 1.5 h / 20 °C
5: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; hydrogen; silver fluoride; potassium carbonate; silver nitrate; triethylamine;
In
tetrahydrofuran; methanol; acetone; acetonitrile;
3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1002/ejoc.201001442
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen; triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
DOI:10.1002/ejoc.201001442
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C
2: N-Bromosuccinimide; silver nitrate / acetone / 1.5 h / 20 °C
3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
4: N-Bromosuccinimide; silver fluoride / acetonitrile / 1.5 h / 20 °C
5: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; hydrogen; triethylamine / tetrahydrofuran / 2 h / 20 °C
With
bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; hydrogen; silver fluoride; silver nitrate; triethylamine; lithium diisopropyl amide;
In
tetrahydrofuran; acetone; acetonitrile;
3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1002/ejoc.201001442