C₁₁H₁₆N₂O₂

Base Information

Chemical Name:C₁₁H₁₆N₂O₂
CAS No.:1357167-23-7
Molecular Formula:C₁₁H₁₆N₂O₂
Molecular Weight:208.26
Hs Code.:

C<sub>11</sub>H<sub>16</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₁H₁₆N₂O₂

Chemical Property:

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Technology Process of C₁₁H₁₆N₂O₂

There total 6 articles about C₁₁H₁₆N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 46010-72-4
aminodurenol

: 1357167-23-7
C₁₁H₁₆N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 1 h / 20 °C

1.2: 0.17 h / 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux

3.1: acetic acid; sodium nitrite / water / 0.17 h / Cooling with ice

With lithium aluminium tetrahydride; acetic anhydride; acetic acid; sodium nitrite; In tetrahydrofuran; water;
DOI:10.1021/ja206744z

Reference yield:

: 99985-81-6
4-Formamino-2.3.5.6-tetramethyl-phenol

: 1357167-23-7
C₁₁H₁₆N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux

2: acetic acid; sodium nitrite / water / 0.17 h / Cooling with ice

With lithium aluminium tetrahydride; acetic acid; sodium nitrite; In tetrahydrofuran; water;
DOI:10.1021/ja206744z

Reference yield:

: 52415-10-8
1-bromo-2,3,5,6-tetramethyl-4-nitrobenzene

: 1357167-23-7
C₁₁H₁₆N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium hydroxide; tert-butyl XPhos / 1,4-dioxane / 24 h / 90 °C / Inert atmosphere

2.1: hydrogen / methanol / 14 h / 20 °C

3.1: acetic anhydride / 1 h / 20 °C

3.2: 0.17 h / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Cooling with ice; Reflux

5.1: acetic acid; sodium nitrite / water / 0.17 h / Cooling with ice

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium aluminium tetrahydride; hydrogen; acetic anhydride; acetic acid; potassium hydroxide; sodium nitrite; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; water;
DOI:10.1021/ja206744z