DANA

Base Information

Chemical Name:DANA
CAS No.:1312705-67-1
Molecular Formula:C₃₆H₅₃IN₂O₆
Molecular Weight:736.731
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of DANA

Chemical Property:

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Technology Process of DANA

There total 16 articles about DANA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1312705-65-9
C₄₂H₅₉IN₂O₆S

: 1312705-67-1
DANA

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -40 °C

2: toluene / 2 h / 60 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2011.03.149

Reference yield:

: C₃₈H₅₆O₉Si

: 1312705-67-1
DANA

Guidance literature:: Multi-step reaction with 14 steps

1.1: dimethylsulfide; boron trifluoride diethyl etherate / 1 h / -20 °C

2.1: dmap; triethylamine / dichloromethane / 16 h / 35 °C

3.1: potassium carbonate / methanol / 3 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 35 °C

5.1: n-butyllithium; diethylaluminium chloride / toluene / 0.33 h / 0 °C

6.1: potassium carbonate / methanol / 2 h / 20 °C

7.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1 h / 20 °C

7.2: 18 h / 20 °C

8.1: Dess-Martin periodane / dichloromethane / 2 h / 30 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C

10.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C

11.1: methanol; acetyl chloride / tetrahydrofuran / 1 h / 0 °C

12.1: ammonia; hydroxylamine-O-sulfonic acid / methanol; dichloromethane / 10 h / 20 °C

12.2: 0.5 h / 0 °C

13.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -40 °C

14.1: toluene / 2 h / 60 °C

With methanol; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; dimethylsulfide; di-isopropyl azodicarboxylate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; ammonia; diethylaluminium chloride; potassium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; hydroxylamine-O-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; 7.1: Sonogashira coupling / 8.1: Dess-Martin oxidation / 10.1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2011.03.149

Reference yield:

: C₃₂H₄₆O₅Si

: 1312705-67-1
DANA

Guidance literature:: Multi-step reaction with 11 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 35 °C

2.1: n-butyllithium; diethylaluminium chloride / toluene / 0.33 h / 0 °C

3.1: potassium carbonate / methanol / 2 h / 20 °C

4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 1 h / 20 °C

4.2: 18 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 2 h / 30 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 50 °C

7.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 1 h / 0 °C

8.1: methanol; acetyl chloride / tetrahydrofuran / 1 h / 0 °C

9.1: ammonia; hydroxylamine-O-sulfonic acid / methanol; dichloromethane / 10 h / 20 °C

9.2: 0.5 h / 0 °C

10.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -40 °C

11.1: toluene / 2 h / 60 °C

With methanol; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; ammonia; diethylaluminium chloride; potassium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; acetyl chloride; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; hydroxylamine-O-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; toluene; 4.1: Sonogashira coupling / 5.1: Dess-Martin oxidation / 7.1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2011.03.149