C₁₂H₁₆BrN₃O₂S

Base Information

Chemical Name:C₁₂H₁₆BrN₃O₂S
CAS No.:1356929-97-9
Molecular Formula:C₁₂H₁₆BrN₃O₂S
Molecular Weight:346.248
Hs Code.:

C<sub>12</sub>H<sub>16</sub>BrN<sub>3</sub>O<sub>2</sub>S

Synonyms:

Suppliers and Price of C₁₂H₁₆BrN₃O₂S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₂H₁₆BrN₃O₂S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₂H₁₆BrN₃O₂S

There total 4 articles about C₁₂H₁₆BrN₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356929-95-7
C₂₄H₃₀Br₂N₆O₄S₂

: 1356929-97-9
C₁₂H₁₆BrN₃O₂S

Guidance literature:: With tris-(2-carboxyethyl)-phosphine hydrochloride; In water; dimethyl sulfoxide; at 25 ℃; for 0.333333h; Darkness;
DOI:10.1021/jm2016182

Reference yield:

: 280140-77-4
4-(3-bromo-4-methoxybenzylidene)-2-methyl-4H-oxazol-5-one

: 1356929-97-9
C₁₂H₁₆BrN₃O₂S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / Reflux

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

3: hydrazine hydrate / methanol / 2.5 h / Reflux

4: tris-(2-carboxyethyl)-phosphine hydrochloride / water; dimethyl sulfoxide / 0.33 h / 25 °C / Darkness

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; tris-(2-carboxyethyl)-phosphine hydrochloride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; water; dimethyl sulfoxide;
DOI:10.1021/jm2016182

Reference yield:

: 34841-06-0
3-bromo-4-methoxybenzylaldehyde

: 1356929-97-9
C₁₂H₁₆BrN₃O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium acetate; acetic anhydride / Reflux

2: hydrogenchloride; water / Reflux

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

4: hydrazine hydrate / methanol / 2.5 h / Reflux

5: tris-(2-carboxyethyl)-phosphine hydrochloride / water; dimethyl sulfoxide / 0.33 h / 25 °C / Darkness

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; sodium acetate; tris-(2-carboxyethyl)-phosphine hydrochloride; acetic anhydride; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; water; dimethyl sulfoxide;
DOI:10.1021/jm2016182