1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen

Base Information

Chemical Name:1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen
CAS No.:123858-43-5
Molecular Formula:C₂₀H₂₉PSi
Molecular Weight:328.51
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen

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Technology Process of 1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen

There total 1 articles about 1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51905-34-1
pentamethylcyclopentadienyllithium

: 82101-81-3,150295-86-6
Bromphosphan

: 123858-43-5,150295-87-7
1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen

Guidance literature:: In Petroleum ether; for 12h;

Reference yield: 85.0%

: 15321-51-4
diiron nonacarbonyl

: 123858-43-5,150295-87-7
1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen

: 150696-02-9
tetracarbonyl{(pentamethylcyclopentadienyl)(phenyl(trimethylsilyl)methylene)phosphane}iron

Guidance literature:: In hexane; addn. of phosphaalkene to Fe complex soln. under inert gas; stirring at room temp. for 3d; filtn., evapn. of volatile compds. in vac., column chromy. of oil in toluene/MeCN (Florisil, toluene); crystn. from pentane at -35°C; elem. anal.;

Reference yield: 75.0%

: 51266-28-5
(Bu₃P)2Ni(cyclo-octa-1,5-diene)

: 123858-43-5,150295-87-7
1-(Pentamethylcyclopentadienyl)-2-phenyl-2-(trimethylsilyl)-phosphaethen

: (η5-pentamethylcyclopentadienyl){phenyl(trimethylsilyl)methylenephosphanyl}(tributylphosphane)nickel

Guidance literature:: In pentane; benzene; dropwise addn. of phosphaalkene to Ni complex soln. under inert gas at -10°C; after 30 min warming to room temp.; stirring for 1h; evapn. of solvent, recrystn. of residue (toluene); elem. anal.;