Technology Process of C22H32O14
There total 7 articles about C22H32O14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; potassium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1055/s-0033-1339338
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve
1.2: 16 h / -40 °C / Inert atmosphere; Molecular sieve
2.1: Acetyl bromide; acetic acid / methanol / 3 h / 20 °C / Inert atmosphere
3.1: tetrabutylammomium bromide; sodium hydroxide / chloroform; water / 6 h / 45 °C / pH 10.5 - 11 / Inert atmosphere
4.1: potassium hydroxide; water / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
With
Acetyl bromide; tetrabutylammomium bromide; water; acetic acid; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; chloroform; water;
DOI:10.1055/s-0033-1339338
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Acetyl bromide; acetic acid / methanol / 3 h / 20 °C / Inert atmosphere
2: tetrabutylammomium bromide; sodium hydroxide / chloroform; water / 6 h / 45 °C / pH 10.5 - 11 / Inert atmosphere
3: potassium hydroxide; water / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
With
Acetyl bromide; tetrabutylammomium bromide; water; acetic acid; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; chloroform; water;
DOI:10.1055/s-0033-1339338
