4-(t-Butyl-diphenyl-silanyloxy)-cyclohexanol

Base Information

Chemical Name:4-(t-Butyl-diphenyl-silanyloxy)-cyclohexanol
CAS No.:130745-64-1
Molecular Formula:C22H30O2Si
Molecular Weight:354.565
Hs Code.:
DSSTox Substance ID:DTXSID601195822

Synonyms:4-(t-butyl-diphenyl-silanyloxy)-cyclohexanol;SCHEMBL241741;SCHEMBL359522;SCHEMBL4797973;LXGBGZOYKCDRQU-UHFFFAOYSA-N;DTXSID601195822;130745-64-1;4-[(tert-butyldiphenylsilyl)oxy]cyclohexan-1-ol;cis-4-[[(1,1-Dimethylethyl)diphenylsilyl]oxy]cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(t-Butyl-diphenyl-silanyloxy)-cyclohexanol

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:354.201506730
Heavy Atom Count:25
Complexity:379

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)[Si](C1=CC=CC=C1)(C2=CC=CC=C2)OC3CCC(CC3)O

Technology Process of 4-(t-Butyl-diphenyl-silanyloxy)-cyclohexanol

There total 2 articles about 4-(t-Butyl-diphenyl-silanyloxy)-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 556-48-9
1,4-Cyclohexanediol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 130745-65-2
trans-4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]cyclohexanol

: 130745-64-1
cis-4-(tert-butyl-diphenylsilyloxy)-cyclohexanol

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 0 ℃; for 1h;

Reference yield:

: 130745-59-4
4-<(tert-Butyldiphenylsilyl)oxy>cyclohexanone

: 130745-65-2
trans-4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]cyclohexanol

: 130745-64-1
cis-4-(tert-butyl-diphenylsilyloxy)-cyclohexanol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; for 0.8h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1246/cl.1990.1507

Reference yield: 71.0%

: 130745-64-1
cis-4-(tert-butyl-diphenylsilyloxy)-cyclohexanol

: 458560-71-9
(S)-3-benzyl-4-methyl-[1,2,3]-oxathiazolidine-2,2-dioxide

: C₃₂H₄₃NO₂Si

Guidance literature:: cis-4-(tert-butyl-diphenylsilyloxy)-cyclohexanol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Cooling with ice;

(S)-3-benzyl-4-methyl-[1,2,3]-oxathiazolidine-2,2-dioxide; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Further stages;