7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone

Base Information

• Chemical Name: 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone
• CAS No.: 129985-41-7
• Molecular Formula: C₄₆H₆₃IO₁₇Si₂
• Molecular Weight: 1071.07

Synonyms:

Chemical Property of 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone

There total 3 articles about 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Epsilon-pyrromycinone (21288-61-9) + 1,5-anhydro-2,6-dideoxy-4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-3-O-(trimethylsilyl)-L-lyxo-hex-1-enitol (129985-40-6) → 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-α-L-talopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6) + 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-α-L-galactopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6) + 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6)

Guidance literature:

With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; Yield given. Multistep reaction. Yields of byproduct given; 1.) a.) CH₂Cl₂, RT, 30 min, b.) 0 deg C, 30 min, 2.) 0 deg C, 20 min;

DOI:10.1021/ja00180a037

Reference yield:

Epsilon-pyrromycinone (21288-61-9) + 1,5-anhydro-2,6-dideoxy-4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-3-O-(trimethylsilyl)-L-lyxo-hex-1-enitol (129985-40-6) → 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-α-L-talopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6) + 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-α-L-galactopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6) + 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6)

Guidance literature:

With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; Yield given. Multistep reaction. Yields of byproduct given; 1.) a.) CH₂Cl₂, RT, 30 min, b.) 0 deg C, 30 min, 2.) 0 deg C, 20 min;

DOI:10.1021/ja00180a037

Reference yield:

Epsilon-pyrromycinone (21288-61-9) + 1,5-anhydro-2,6-dideoxy-4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-3-O-(trimethylsilyl)-L-lyxo-hex-1-enitol (129985-40-6) → 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-α-L-talopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6) + 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-α-L-galactopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6) + 7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-3-O-(trimethylsilyl)-β-L-galactopyranosyl>-ε-pyrromycinone (129985-41-7,130061-12-0,143396-45-6)

Guidance literature:

With iodonium(di-γ-collidine) perchlorate; 4 A molecular sieve; Yield given. Multistep reaction. Yields of byproduct given; 1.) a.) CH₂Cl₂, RT, 30 min, b.) 0 deg C, 30 min, 2.) 0 deg C, 20 min;

DOI:10.1021/ja00180a037

upstream raw materials:

Epsilon-pyrromycinone

1,5-anhydro-2,6-dideoxy-4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-3-O-(trimethylsilyl)-α-L-lyxo-hexopyranosyl>-3-O-(trimethylsilyl)-L-lyxo-hex-1-enitol

Downstream raw materials:

ciclamycin 0

7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-α-L-talopyranosyl>-ε-pyrromycinone

7-O-<4-O-<4-O-(2,3,6-trideoxy-α-L-glycero-hexopyranosid-4-ulosyl)-2,6-dideoxy-α-L-lyxo-hexopyranosyl>-2,6-dideoxy-2-iodo-α-L-galactopyranosyl>-ε-pyrromycinone

C₄₀H₄₇IO₁₇

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