C₄₇H₄₃NO₄P₂

Base Information

• Chemical Name: C₄₇H₄₃NO₄P₂
• CAS No.: 1334163-40-4
• Molecular Formula: C₄₇H₄₃NO₄P₂
• Molecular Weight: 747.81
• Mol file: 1334163-40-4.mol

Synonyms:

Chemical Property of C₄₇H₄₃NO₄P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₄₃NO₄P₂

There total 1 articles about C₄₇H₄₃NO₄P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

C31H43OPSn (1222989-89-0) + N-Boc-2,5-diiodopyrrole (117657-44-0) → C47H43NO4P2 (1334163-40-4) + C47H43NO4P2

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; trifuran-2-yl-phosphane; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h; optical yield given as %de; Inert atmosphere;

DOI:10.1002/hc.20708

Reference yield: 42.0%

C47H43NO4P2 (1334163-40-4) → C42H35NP2S2 (1334163-42-6)

Guidance literature:

With Lawessons reagent; In toluene; for 3h; Inert atmosphere; Reflux;

DOI:10.1002/hc.20708

Reference yield:

C47H43NO4P2 (1334163-40-4) → C42H35NP2 (1334163-44-8) + C42H35NP2

Guidance literature:

Multi-step reaction with 2 steps

1: Lawessons reagent / toluene / 3 h / Inert atmosphere; Reflux

2: Hexamethylphosphorous triamide / toluene / 1 h / Inert atmosphere; Reflux

With Lawessons reagent; Hexamethylphosphorous triamide; In toluene;

DOI:10.1002/hc.20708

upstream raw materials:

C₃₁H₄₃OPSn

N-Boc-2,5-diiodopyrrole

Downstream raw materials:

C₄₂H₃₅NP₂S₂

C₄₂H₃₅NP₂