(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury⁽¹⁺⁾ salt

Base Information

• Chemical Name: (S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury⁽¹⁺⁾ salt
• CAS No.: 49841-82-9
• Molecular Formula: 2C₂H₃O₂*C₁₆H₁₆N₂O₄S*2Hg
• Molecular Weight: 851.649

Synonyms:

Chemical Property of (S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury⁽¹⁺⁾ salt

Chemical Property:

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Technology Process of (S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury⁽¹⁺⁾ salt

There total 1 articles about (S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury⁽¹⁺⁾ salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury(1+) salt (49841-82-9)

Guidance literature:

K-benzylpenicillinat,Hg(OAc)2,HOAc;

DOI:10.1039/c39730000477

Reference yield:

(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury(1+) salt (49841-82-9) → (S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid

Guidance literature:

With pyridine;

DOI:10.1039/P19740000181

Reference yield:

(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; bis-acetatomercury(1+) salt (49841-82-9) → (1S,5R)-3-benzyl-6-(2-methylprop-1-enyl)-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-7-one (49841-83-0)

Guidance literature:

With dimethyl sulfoxide;

DOI:10.1039/P19740000181

Downstream raw materials:

N-(2-benzyl-oxazole-4-carbonyl)-D-penicillamine methyl ester

N-[(5S)-2c-(1-mercapto-1-methyl-ethyl)-3,7-dioxo-(5rH)-4-oxa-1-aza-bicyclo[3.2.0]hept-6c-yl]-2-phenyl-acetamide

(S)-2-((1S)-3-benzyl-7-oxo-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid methyl ester

(1S,5R)-3-benzyl-6-(2-methylprop-1-enyl)-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-7-one

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