N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide

Base Information

Chemical Name:N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide
CAS No.:1187086-62-9
Molecular Formula:C₂₄H₂₅ClNOPSi
Molecular Weight:437.981
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide

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Technology Process of N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide

There total 1 articles about N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849940-62-1
C₁₉H₁₅ClNOP

: 1066-54-2
trimethylsilylacetylene

: 1187086-62-9
N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide

: N-(1-(3-chlorophenyl)-3-(trimethylsilyl)prop-2-ynyl)-P,P-diphenylphosphiic amide

Guidance literature:: trimethylsilylacetylene; With (2S,2S')-1,1'-(5-methyl-1,3-phenylene)bis(methylene)bis(pyrrolidin-2-ylmethanol); diethylzinc; In toluene; for 7h; Inert atmosphere;

C₁₉H₁₅ClNOP; In toluene; at 0 - 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/jo901492w