tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-β-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside

Base Information

• Chemical Name: tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-β-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside
• CAS No.: 1040282-44-7
• Molecular Formula: C₅₆H₇₉N₃O₁₁Si₂
• Molecular Weight: 1026.43
• Mol file: 1040282-44-7.mol

Synonyms:

Chemical Property of tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-β-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-β-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside

There total 1 articles about tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-β-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H37N3O5Si + C38H50O9Si (1040282-31-2) → tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-β-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside (1040282-44-7) + tert-butyldimethylsilyl 2-azido-3,6-di-O-benzyl-4-O-[2-O-benzyl-4,6-O-benzylidene-3-O-tri-iso-propylsilyloxy-methyl-α-D-mannopyranosyl]-2-deoxy-β-D-glucopyranoside (1040282-45-8)

Guidance literature:

C₂₆H₃₇N₃O₅Si; With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -40 - 25 ℃; Molecular sieve;

C₃₈H₅₀O₉Si; In dichloromethane; at -25 - 20 ℃; optical yield given as %de;

DOI:10.1002/chem.200701864

upstream raw materials:

C₃₈H₅₀O₉Si