Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2

Base Information

Chemical Name:Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2
CAS No.:1244340-88-2
Molecular Formula:C₅₇H₇₈Al₃N₅
Molecular Weight:914.224
Hs Code.:

Al<sub>3</sub>(CH<sub>3</sub>)3(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)3(NCC<sub>6</sub>H<sub>3</sub>(CH<sub>3</sub>)2)2

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Suppliers and Price of Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2

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Chemical Property of Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2

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Technology Process of Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2

There total 2 articles about Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 117960-70-0
tris[μ-[2,6-bis(1-methylethyl)benzenaminato]]trimethyltricycloaluminum

: 6575-13-9
2,6-dimethylbenzonitrile

: 1244340-88-2
Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2

Guidance literature:: In toluene; (N2) mixt. Al complex and nitrile in toluene was stirred at room temp. for 1 h; soln. was filtered, volatiles were removed in vacuo, residue was dissolved in hexane, ppt. was filtered off and washed with cold hexane;
DOI:10.1021/om100406y

Reference yield: 43.0%

: [(2,6-diisopropylphenyl)HNAlMe₂]2

: 6575-13-9
2,6-dimethylbenzonitrile

: Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)

: 1244340-88-2
Al₃(CH₃)3(NC₆H₃(CH(CH₃)2)2)3(NCC₆H₃(CH₃)2)2

Guidance literature:: In neat (no solvent); mixt. Al complex and nitrile was heated at 170°C for 3 h; react. mixt. was cooled to room temp., residue was dissolved in hexane, filtered through Celite and left at room temp.; elem. anal.;
DOI:10.1021/om100406y