C₂₂H₂₂F₄N₂

Base Information

Chemical Name:C₂₂H₂₂F₄N₂
CAS No.:1166846-91-8
Molecular Formula:C₂₂H₂₂F₄N₂
Molecular Weight:390.424
Hs Code.:

C<sub>22</sub>H<sub>22</sub>F<sub>4</sub>N<sub>2</sub>

Synonyms:

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Chemical Property of C₂₂H₂₂F₄N₂

Chemical Property:

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Technology Process of C₂₂H₂₂F₄N₂

There total 6 articles about C₂₂H₂₂F₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-[(4-fluoro-phenyl)-hydrazono]-cyclohexanone

: 1166846-91-8
C₂₂H₂₂F₄N₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: phosphoric acid; acetic acid / 12 h / 75 °C / Inert atmosphere

2.1: hydroxylamine hydrochloride / ethanol; water / 12 h / Darkness

3.1: PPA / 2 h / 90 - 100 °C

4.1: lithium aluminium tetrahydride / 1,4-dioxane / 8 h

5.1: ethanol; water / 0.5 h / 20 °C

5.2: 48 h / 20 °C

6.1: tetrabutylammonium sulfate; potassium hydroxide / water; dimethyl sulfoxide / 80 °C

7.1: platinum(IV) oxide; hydrogen / ethanol / 20 °C / 760.05 Torr

With platinum(IV) oxide; lithium aluminium tetrahydride; phosphoric acid; hydroxylamine hydrochloride; hydrogen; acetic acid; tetrabutylammonium sulfate; potassium hydroxide; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide;
DOI:10.2174/157018010791306579

Reference yield:

: 919120-68-6
9-fluoro-1,2,3,4,5,6-hexahydroazepino[4,3-b]indole

: 1166846-91-8
C₂₂H₂₂F₄N₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol; water / 0.5 h / 20 °C

1.2: 48 h / 20 °C

2.1: tetrabutylammonium sulfate; potassium hydroxide / water; dimethyl sulfoxide / 80 °C

3.1: platinum(IV) oxide; hydrogen / ethanol / 20 °C / 760.05 Torr

With platinum(IV) oxide; hydrogen; tetrabutylammonium sulfate; potassium hydroxide; In ethanol; water; dimethyl sulfoxide;
DOI:10.2174/157018010791306579

Reference yield:

: 1009631-55-3
2-methyl-9-fluoro-1,2,3,4,5,6-hexahydroazepino[4,3-b]indole

: 1166846-91-8
C₂₂H₂₂F₄N₂

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium sulfate; potassium hydroxide / water; dimethyl sulfoxide / 80 °C

2: platinum(IV) oxide; hydrogen / ethanol / 20 °C / 760.05 Torr

With platinum(IV) oxide; hydrogen; tetrabutylammonium sulfate; potassium hydroxide; In ethanol; water; dimethyl sulfoxide;
DOI:10.2174/157018010791306579