Technology Process of C10H9N5O3
There total 4 articles about C10H9N5O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / tetrahydrofuran
2: sodium carbonate / tetrahydrofuran / Reflux
3: hydrazine hydrate / 1 h / 90 °C
4: sulfuric acid / 4 h / 20 °C
With
sulfuric acid; sodium hydride; sodium carbonate; hydrazine hydrate;
In
tetrahydrofuran;
DOI:10.2174/1570180811666140115234123
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / tetrahydrofuran / Reflux
2: hydrazine hydrate / 1 h / 90 °C
3: sulfuric acid / 4 h / 20 °C
With
sulfuric acid; sodium carbonate; hydrazine hydrate;
In
tetrahydrofuran;
DOI:10.2174/1570180811666140115234123
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / Reflux
2: sodium hydride / tetrahydrofuran
3: sodium carbonate / tetrahydrofuran / Reflux
4: hydrazine hydrate / 1 h / 90 °C
5: sulfuric acid / 4 h / 20 °C
With
thionyl chloride; sulfuric acid; sodium hydride; sodium carbonate; hydrazine hydrate;
In
tetrahydrofuran;
DOI:10.2174/1570180811666140115234123