1-Decene, 2-fluoro-

Base Information

• Chemical Name: 1-Decene, 2-fluoro-
• CAS No.: 130876-17-4
• Molecular Formula: C10H19F
• Molecular Weight: 158.259
• DSSTox Substance ID: DTXSID10456493
• Nikkaji Number: J2.904.082F
• Wikidata: Q82279024

Synonyms:1-Decene, 2-fluoro-;130876-17-4;2-Fluoro-1-decene;SCHEMBL9797560;DTXSID10456493

Chemical Property of 1-Decene, 2-fluoro-

Chemical Property:

• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 7
• Exact Mass: 158.147078768
• Heavy Atom Count: 11
• Complexity: 97

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCC(=C)F

Technology Process of 1-Decene, 2-fluoro-

There total 4 articles about 1-Decene, 2-fluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1-decenyl(p-trifluoromethylphenyl)-λ(3)-bromane → 1-decyne (764-93-2) + p-trifluoromethylphenyl bromide (402-43-7) + α-fluorodec-1-en (130876-17-4) + (Z)-1-decenyl fluoride (66291-49-4)

Guidance literature:

In dichloromethane; at -78 - 0 ℃; for 3h; Inert atmosphere;

DOI:10.1021/ja200479p

Reference yield:

1-Decene (872-05-9,17438-89-0,25189-70-2) → 1-fluorodecene + 1-decyne (764-93-2) + α-fluorodec-1-en (130876-17-4)

Guidance literature:

1-Decene; With N-Bromosuccinimide; triethylamine hydrofluoride; In dichloromethane; at 0 - 20 ℃;

With potassium tert-butylate; In pentane; for 5h; Heating;

DOI:10.1016/j.jfluchem.2004.09.001

Reference yield:

potassium (E)-1-decenyltrifluoroborate → 1-decyne (764-93-2) + α-fluorodec-1-en (130876-17-4) + (Z)-1-decenyl fluoride (66291-49-4)

Guidance literature:

Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

2: dichloromethane / 1 h / -78 °C / Inert atmosphere

3: dichloromethane / 3 h / -78 - 0 °C / Inert atmosphere

With boron trifluoride diethyl etherate; In dichloromethane;

DOI:10.1021/ja200479p

upstream raw materials:

1-Decene

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