C₂₁H₂₃ClO₅

Base Information

Chemical Name:C₂₁H₂₃ClO₅
CAS No.:1327165-98-9
Molecular Formula:C₂₁H₂₃ClO₅
Molecular Weight:390.864
Hs Code.:

C<sub>21</sub>H<sub>23</sub>ClO<sub>5</sub>

Synonyms:

Suppliers and Price of C₂₁H₂₃ClO₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₃ClO₅

Chemical Property:

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Technology Process of C₂₁H₂₃ClO₅

There total 12 articles about C₂₁H₂₃ClO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1185339-52-9
C₂₉H₃₁ClO₉

: 1327165-98-9
C₂₁H₂₃ClO₅

Guidance literature:: With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 1185339-44-9
C₁₉H₂₁ClO₅

: 1327165-98-9
C₂₁H₂₃ClO₅

Guidance literature:: Multi-step reaction with 5 steps

1: dmap / pyridine; dichloromethane / 20 °C

2: aluminum (III) chloride / dichloromethane / 0 - 20 °C

3: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

4: toluene-4-sulfonic acid / water; toluene / Reflux

5: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 20 °C

With dmap; aluminum (III) chloride; sodium tetrahydroborate; lithium hydroxide monohydrate; water; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; toluene; 2: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 312749-31-8
2-chloro-5-bromobenzophenone

: 1327165-98-9
C₂₁H₂₃ClO₅

Guidance literature:: Multi-step reaction with 9 steps

1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / Reflux

2: n-butyllithium / tetrahydrofuran; toluene / -78 °C

3: methanesulfonic acid / methanesulfonic acid / -78 - 20 °C

4: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -30 - -10 °C

5: dmap / pyridine; dichloromethane / 20 °C

6: aluminum (III) chloride / dichloromethane / 0 - 20 °C

7: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

8: toluene-4-sulfonic acid / water; toluene / Reflux

9: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 20 °C

With triethylsilane; dmap; aluminum (III) chloride; sodium tetrahydroborate; n-butyllithium; methanesulfonic acid; lithium hydroxide monohydrate; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; water; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; methanesulfonic acid; dichloromethane; water; toluene; acetonitrile; 6: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032