Technology Process of C23H33N3O2
There total 3 articles about C23H33N3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 10 h
2: sodium cyanoborohydride / 1,2-dichloro-ethane / 2 h / 20 °C / Inert atmosphere
With
sodium cyanoborohydride; trifluoroacetic acid;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2011.09.057
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with acetone-dry ice
2: trifluoroacetic acid / dichloromethane / 10 h
3: sodium cyanoborohydride / 1,2-dichloro-ethane / 2 h / 20 °C / Inert atmosphere
With
sodium cyanoborohydride; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2011.09.057
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / 1,4-dioxane; water / 15 h
2: tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with acetone-dry ice
3: trifluoroacetic acid / dichloromethane / 10 h
4: sodium cyanoborohydride / 1,2-dichloro-ethane / 2 h / 20 °C / Inert atmosphere
With
sodium cyanoborohydride; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/j.bmcl.2011.09.057