C₃₄H₄₀N₅O₈PS₂

Base Information

Chemical Name:C₃₄H₄₀N₅O₈PS₂
CAS No.:1277171-65-9
Molecular Formula:C₃₄H₄₀N₅O₈PS₂
Molecular Weight:741.826
Hs Code.:

C<sub>34</sub>H<sub>40</sub>N<sub>5</sub>O<sub>8</sub>PS<sub>2</sub>

Synonyms:

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Chemical Property of C₃₄H₄₀N₅O₈PS₂

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Technology Process of C₃₄H₄₀N₅O₈PS₂

There total 4 articles about C₃₄H₄₀N₅O₈PS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1277171-56-8
C₂₇H₂₉N₅O₇

: 198637-74-0
2-chloro-“spiro”-4,4-pentamethylene-1,3,2-oxathiaphospholane

: 1277171-65-9
C₃₄H₄₀N₅O₈PS₂

Guidance literature:: C₂₇H₂₉N₅O₇; 2-chloro-“spiro”-4,4-pentamethylene-1,3,2-oxathiaphospholane; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

With sulfur; In dichloromethane; for 24h;
DOI:10.1002/chir.20905

Reference yield:

: 39637-74-6
(1S)-(-)-camphanic chloride

: 1277171-65-9
C₃₄H₄₀N₅O₈PS₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / 5 h / 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol; chloroform / 0.33 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

3.2: 24 h

With pyridine; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; chloroform;
DOI:10.1002/chir.20905

Reference yield:

: 1277171-48-8
C₄₈H₄₇N₅O₉

: 1277171-65-9
C₃₄H₄₀N₅O₈PS₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / methanol; chloroform / 0.33 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

2.2: 24 h

With toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; chloroform;
DOI:10.1002/chir.20905