Technology Process of C23H40O8Si
There total 9 articles about C23H40O8Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
dichloromethane; water;
at 0 ℃;
for 0.333333h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -40 °C
1.2: 1 h / 0 °C
2.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C
2.2: 2.17 h / -78 °C
2.3: -78 - 20 °C
3.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C
4.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C
5.1: 1H-imidazole / dichloromethane / 1 h / 20 °C
6.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C
6.2: 1 h / 0 - 20 °C
7.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C
8.1: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere
9.1: sodium hydrogencarbonate / dichloromethane; water / 0.33 h / 0 °C / Inert atmosphere
With
1H-imidazole; dmap; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; sodium hydrogencarbonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; acetonitrile;
8.1: Pummerer reaction;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C
1.2: 2.17 h / -78 °C
1.3: -78 - 20 °C
2.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C
3.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C
4.1: 1H-imidazole / dichloromethane / 1 h / 20 °C
5.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C
5.2: 1 h / 0 - 20 °C
6.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 6 h / 0 - 20 °C
7.1: triethylamine / dichloromethane / 0.25 h / 0 °C / Inert atmosphere
8.1: sodium hydrogencarbonate / dichloromethane; water / 0.33 h / 0 °C / Inert atmosphere
With
1H-imidazole; dmap; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; sodium hydrogencarbonate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; zinc(II) chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile;
7.1: Pummerer reaction;
